TY - JOUR
T1 - X-ray directional dark-field imaging using Unified Modulated Pattern Analysis
AU - Smith, Ronan
AU - De Marco, Fabio
AU - Broche, Ludovic
AU - Zdora, Marie Christine
AU - Phillips, Nicholas W.
AU - Boardman, Richard
AU - Thibault, Pierre
N1 - Funding Information:
PT received funding from the European Union’s Horizon 2020 research and innovation program (grant agreement no. 866026). NP received funding from the European Union’s Horizon 2020 research and innovation program under the Marie Skłodowska-Curie grant agreement No. 884104. The funders had no role in study design, data collection and analysis, decision to publish, or preparation of the manuscript. We thank Irene Zanette for experimental assistance. We thank Vittorio Di Trapani, Sara Savatović, Marco Margini and Ginevra Lautizi for providing insightful discussion. We acknowledge the European Synchrotron Radiation Facility for provision of synchrotron radiation facilities and we would like to thank Alexander Rack for assistance in using beamline ID19.
Publisher Copyright:
© 2022 Smith et al. This is an open access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited.
PY - 2022/8/29
Y1 - 2022/8/29
N2 - X-ray directional dark-field imaging is a recent technique that can reveal a sample’s small-scale structural properties which are otherwise invisible in a conventional imaging system. In particular, directional dark-field can detect and quantify the orientation of anisotropic structures. Here, we present an algorithm that allows for the extraction of a directional dark-field signal from X-ray speckle-based imaging data. The experimental setup is simple, as it requires only the addition of a diffuser to a full-field microscope setup. Sandpaper is an appropriate diffuser material in the hard x-ray regime. We propose an approach to extract the mean scattering width, directionality, and orientation from the recorded speckle images acquired with the technique. We demonstrate that our method can detect and quantify the orientation of fibres inside a carbon fibre reinforced polymer (CFRP) sample within one degree of accuracy and show how the accuracy depends on the number of included measurements. We show that the reconstruction parameters can be tuned to increase or decrease accuracy at the expense of spatial resolution.
AB - X-ray directional dark-field imaging is a recent technique that can reveal a sample’s small-scale structural properties which are otherwise invisible in a conventional imaging system. In particular, directional dark-field can detect and quantify the orientation of anisotropic structures. Here, we present an algorithm that allows for the extraction of a directional dark-field signal from X-ray speckle-based imaging data. The experimental setup is simple, as it requires only the addition of a diffuser to a full-field microscope setup. Sandpaper is an appropriate diffuser material in the hard x-ray regime. We propose an approach to extract the mean scattering width, directionality, and orientation from the recorded speckle images acquired with the technique. We demonstrate that our method can detect and quantify the orientation of fibres inside a carbon fibre reinforced polymer (CFRP) sample within one degree of accuracy and show how the accuracy depends on the number of included measurements. We show that the reconstruction parameters can be tuned to increase or decrease accuracy at the expense of spatial resolution.
UR - https://www.scopus.com/pages/publications/85136875154
U2 - 10.1371/journal.pone.0273315
DO - 10.1371/journal.pone.0273315
M3 - Article
C2 - 36037163
AN - SCOPUS:85136875154
SN - 1932-6203
VL - 17
JO - PLoS ONE
JF - PLoS ONE
IS - 8
M1 - e0273315
ER -