Understanding the effects of PBF process parameter interplay on Ti-6Al-4V surface properties

Trina Majumdar, Tiphaine Bazin, Emily Massahud Carvalho Ribeiro, Jessica Ellen Frith, Nick Birbilis

Research output: Contribution to journalArticleResearchpeer-review

Abstract

Ti-6Al-4V is commonly used in orthopaedic implants, and fabrication techniques such as Powder Bed Fusion (PBF) are becoming increasingly popular for the net-shape production of such implants, as PBF allows for complex customisation and minimal material wastage. Present research into PBF fabricated Ti-6Al-4V focuses on new design strategies (e.g. designing pores, struts or lattices) or mechanical property optimisation through process parameter control–however, it is pertinent to examine the effects of altering PBF process parameters on properties relating to bioactivity. Herein, changes in Ti-6Al-4V microstructure, mechanical properties and surface characteristics were examined as a result of varying PBF process parameters, with a view to understanding how to tune Ti-6Al-4V bio-activity during the fabrication stage itself. The interplay between various PBF laser scan speeds and laser powers influenced Ti-6Al-4V hardness, porosity, roughness and corrosion resistance, in a manner not clearly described by the commonly used volumetric energy density (VED) design variable. Key findings indicate that the relationships between PBF process parameters and ultimate Ti-6Al-4V properties are not straightforward as expected, and that wide ranges of porosity (0.03 ± 0.01% to 32.59 ± 2.72%) and corrosion resistance can be achieved through relatively minor changes in process parameters used–indicating volumetric energy density is a poor predictor of PBF Ti-6Al-4V properties. While variations in electrochemical behaviour with respect to the process parameters used in the PBF fabrication of Ti-6Al-4V have previously been reported, this study presents data regarding important surface characteristics over a large process window, reflecting the full capabilities of current PBF machinery.

Original languageEnglish
Article numbere0221198
Number of pages24
JournalPLoS ONE
Volume14
Issue number8
DOIs
Publication statusPublished - 29 Aug 2019

Cite this

Majumdar, Trina ; Bazin, Tiphaine ; Ribeiro, Emily Massahud Carvalho ; Frith, Jessica Ellen ; Birbilis, Nick. / Understanding the effects of PBF process parameter interplay on Ti-6Al-4V surface properties. In: PLoS ONE. 2019 ; Vol. 14, No. 8.
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abstract = "Ti-6Al-4V is commonly used in orthopaedic implants, and fabrication techniques such as Powder Bed Fusion (PBF) are becoming increasingly popular for the net-shape production of such implants, as PBF allows for complex customisation and minimal material wastage. Present research into PBF fabricated Ti-6Al-4V focuses on new design strategies (e.g. designing pores, struts or lattices) or mechanical property optimisation through process parameter control–however, it is pertinent to examine the effects of altering PBF process parameters on properties relating to bioactivity. Herein, changes in Ti-6Al-4V microstructure, mechanical properties and surface characteristics were examined as a result of varying PBF process parameters, with a view to understanding how to tune Ti-6Al-4V bio-activity during the fabrication stage itself. The interplay between various PBF laser scan speeds and laser powers influenced Ti-6Al-4V hardness, porosity, roughness and corrosion resistance, in a manner not clearly described by the commonly used volumetric energy density (VED) design variable. Key findings indicate that the relationships between PBF process parameters and ultimate Ti-6Al-4V properties are not straightforward as expected, and that wide ranges of porosity (0.03 ± 0.01{\%} to 32.59 ± 2.72{\%}) and corrosion resistance can be achieved through relatively minor changes in process parameters used–indicating volumetric energy density is a poor predictor of PBF Ti-6Al-4V properties. While variations in electrochemical behaviour with respect to the process parameters used in the PBF fabrication of Ti-6Al-4V have previously been reported, this study presents data regarding important surface characteristics over a large process window, reflecting the full capabilities of current PBF machinery.",
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Understanding the effects of PBF process parameter interplay on Ti-6Al-4V surface properties. / Majumdar, Trina; Bazin, Tiphaine; Ribeiro, Emily Massahud Carvalho; Frith, Jessica Ellen; Birbilis, Nick.

In: PLoS ONE, Vol. 14, No. 8, e0221198, 29.08.2019.

Research output: Contribution to journalArticleResearchpeer-review

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