Synthesis of highly ordered large-pore mesoporous organosilicas by non-aqueous solvent evaporation method

Zhen Dong Zhang; Xiao Xia Yan; Bo Zhi Tian; Shao Dian Shen; De Hong Chen; Qian Rong Fang; Guang Shan Zhu; Shi Lun Qiu; Dong Yuan Zhao

Synthesis of highly ordered large-pore mesoporous organosilicas by non-aqueous solvent evaporation method

Zhen Dong Zhang, Xiao Xia Yan, Bo Zhi Tian, Shao Dian Shen, De Hong Chen, Qian Rong Fang, Guang Shan Zhu, Shi Lun Qiu, Dong Yuan Zhao

Research output: Contribution to journal › Article › Research › peer-review

1 Citation (Scopus)

Abstract

Highly ordered hexagonal mesoporous organosilicas with large pore size > 4 nm) were synthesized by non-aqueous solvent evaporation method using triblock copolymers as the structure-directing a-gents and 1,2-bis(triethoxysilyl)ethane as the organically bridged silica source. The mesoprous organosilicas were characterized by small-angle powder X ray diffraction(XRD), transmission electron microscopy (TEM), nitrogen adsorption, ²⁹Si MAS NMR spectroscopy and scanning electron microscope(SEM).

Original language	English
Pages (from-to)	603-606
Number of pages	4
Journal	Chemical Journal of Chinese Universities
Volume	26
Issue number	4
Publication status	Published - 1 Apr 2005
Externally published	Yes

Keywords

Mesoporous organosilica material
Non-aqueous solvent evaporation
Synthesis

Cite this

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title = "Synthesis of highly ordered large-pore mesoporous organosilicas by non-aqueous solvent evaporation method",

abstract = "Highly ordered hexagonal mesoporous organosilicas with large pore size > 4 nm) were synthesized by non-aqueous solvent evaporation method using triblock copolymers as the structure-directing a-gents and 1,2-bis(triethoxysilyl)ethane as the organically bridged silica source. The mesoprous organosilicas were characterized by small-angle powder X ray diffraction(XRD), transmission electron microscopy (TEM), nitrogen adsorption, 29Si MAS NMR spectroscopy and scanning electron microscope(SEM).",

keywords = "Mesoporous organosilica material, Non-aqueous solvent evaporation, Synthesis",

author = "Zhang, {Zhen Dong} and Yan, {Xiao Xia} and Tian, {Bo Zhi} and Shen, {Shao Dian} and Chen, {De Hong} and Fang, {Qian Rong} and Zhu, {Guang Shan} and Qiu, {Shi Lun} and Zhao, {Dong Yuan}",

year = "2005",

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day = "1",

language = "English",

volume = "26",

pages = "603--606",

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T1 - Synthesis of highly ordered large-pore mesoporous organosilicas by non-aqueous solvent evaporation method

AU - Zhang, Zhen Dong

AU - Yan, Xiao Xia

AU - Tian, Bo Zhi

AU - Shen, Shao Dian

AU - Chen, De Hong

AU - Fang, Qian Rong

AU - Zhu, Guang Shan

AU - Qiu, Shi Lun

AU - Zhao, Dong Yuan

PY - 2005/4/1

Y1 - 2005/4/1

N2 - Highly ordered hexagonal mesoporous organosilicas with large pore size > 4 nm) were synthesized by non-aqueous solvent evaporation method using triblock copolymers as the structure-directing a-gents and 1,2-bis(triethoxysilyl)ethane as the organically bridged silica source. The mesoprous organosilicas were characterized by small-angle powder X ray diffraction(XRD), transmission electron microscopy (TEM), nitrogen adsorption, 29Si MAS NMR spectroscopy and scanning electron microscope(SEM).

AB - Highly ordered hexagonal mesoporous organosilicas with large pore size > 4 nm) were synthesized by non-aqueous solvent evaporation method using triblock copolymers as the structure-directing a-gents and 1,2-bis(triethoxysilyl)ethane as the organically bridged silica source. The mesoprous organosilicas were characterized by small-angle powder X ray diffraction(XRD), transmission electron microscopy (TEM), nitrogen adsorption, 29Si MAS NMR spectroscopy and scanning electron microscope(SEM).

KW - Mesoporous organosilica material

KW - Non-aqueous solvent evaporation

KW - Synthesis

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M3 - Article

AN - SCOPUS:17944367063

SN - 0251-0790

VL - 26

SP - 603

EP - 606

JO - Chemical Journal of Chinese Universities

JF - Chemical Journal of Chinese Universities

IS - 4

ER -

Synthesis of highly ordered large-pore mesoporous organosilicas by non-aqueous solvent evaporation method

Abstract

Keywords

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