Oxidised compounds in aviation fuels using Nafion fibre solid phase microextraction

R L Webster; J. B. Mete; P. M. Rawson; D J Evans; P J Marriott

doi:10.1016/j.fuel.2017.02.031

Oxidised compounds in aviation fuels using Nafion fibre solid phase microextraction

R L Webster, J. B. Mete, P. M. Rawson, D J Evans, P J Marriott

School of Chemistry

Research output: Contribution to journal › Article › Research › peer-review

5 Citations (Scopus)

Abstract

Nafion solid phase microextraction fibres were prepared and applied to the analysis of polar oxygenated analytes in non-polar aviation fuel matrices. The performance of the Nafion fibres was investigated and exhibited higher extraction efficiencies for polar analytes spiked into a reference non-polar fuel, compared with a commercially available polar (Carbowax) phase fibre. Oxygen-containing compounds were also tentatively identified in thermally oxidised aviation fuels using both single column and multidimensional gas chromatography with mass spectrometry.

Original language	English
Pages (from-to)	226-231
Number of pages	6
Journal	Fuel
Volume	197
DOIs	https://doi.org/10.1016/j.fuel.2017.02.031
Publication status	Published - 1 Jun 2017

Keywords

Alternate fuels
Fuel thermal oxidation
Multidimensional gas chromatography
Nafion
Solid phase microextraction SPME

Access to Document

10.1016/j.fuel.2017.02.031

Link to publication in Scopus

Cite this

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title = "Oxidised compounds in aviation fuels using Nafion fibre solid phase microextraction",

abstract = "Nafion solid phase microextraction fibres were prepared and applied to the analysis of polar oxygenated analytes in non-polar aviation fuel matrices. The performance of the Nafion fibres was investigated and exhibited higher extraction efficiencies for polar analytes spiked into a reference non-polar fuel, compared with a commercially available polar (Carbowax) phase fibre. Oxygen-containing compounds were also tentatively identified in thermally oxidised aviation fuels using both single column and multidimensional gas chromatography with mass spectrometry.",

keywords = "Alternate fuels, Fuel thermal oxidation, Multidimensional gas chromatography, Nafion, Solid phase microextraction SPME",

author = "Webster, {R L} and Mete, {J. B.} and Rawson, {P. M.} and Evans, {D J} and Marriott, {P J}",

year = "2017",

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doi = "10.1016/j.fuel.2017.02.031",

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AU - Webster, R L

AU - Mete, J. B.

AU - Rawson, P. M.

AU - Evans, D J

AU - Marriott, P J

PY - 2017/6/1

Y1 - 2017/6/1

N2 - Nafion solid phase microextraction fibres were prepared and applied to the analysis of polar oxygenated analytes in non-polar aviation fuel matrices. The performance of the Nafion fibres was investigated and exhibited higher extraction efficiencies for polar analytes spiked into a reference non-polar fuel, compared with a commercially available polar (Carbowax) phase fibre. Oxygen-containing compounds were also tentatively identified in thermally oxidised aviation fuels using both single column and multidimensional gas chromatography with mass spectrometry.

AB - Nafion solid phase microextraction fibres were prepared and applied to the analysis of polar oxygenated analytes in non-polar aviation fuel matrices. The performance of the Nafion fibres was investigated and exhibited higher extraction efficiencies for polar analytes spiked into a reference non-polar fuel, compared with a commercially available polar (Carbowax) phase fibre. Oxygen-containing compounds were also tentatively identified in thermally oxidised aviation fuels using both single column and multidimensional gas chromatography with mass spectrometry.

KW - Alternate fuels

KW - Fuel thermal oxidation

KW - Multidimensional gas chromatography

KW - Nafion

KW - Solid phase microextraction SPME

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