Microwave-assisted synthesis of organically functionalized hexa-molybdovanadates

H. Karoui; C. Ritchie

doi:10.1039/c7nj02820b

Microwave-assisted synthesis of organically functionalized hexa-molybdovanadates

H. Karoui, C. Ritchie

Research output: Contribution to journal › Article › Research › peer-review

13 Citations (Scopus)

Abstract

The microwave-assisted reaction of (TBA)₄[β-Mo₈O₂₄] and (TBA)₃[H₃V₁₀O₂₈] with pentaerythritol or tris(hydroxymethyl)aminomethane yields polyanions with the general formula (TBA)₂[V₃Mo₃O₁₆(O₃-R)] (R: C₅H₈OH-1; R: C₄H₆NH₂-3). Post-synthetic esterification of 1 yields the acylated derivative 2, with all compounds being characterized in the solid and solution state.

Original language	English
Pages (from-to)	25-28
Number of pages	4
Journal	New Journal of Chemistry
Volume	42
Issue number	1
DOIs	https://doi.org/10.1039/c7nj02820b
Publication status	Published - 7 Jan 2018
Externally published	Yes

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title = "Microwave-assisted synthesis of organically functionalized hexa-molybdovanadates",

abstract = "The microwave-assisted reaction of (TBA)4[β-Mo8O24] and (TBA)3[H3V10O28] with pentaerythritol or tris(hydroxymethyl)aminomethane yields polyanions with the general formula (TBA)2[V3Mo3O16(O3-R)] (R: C5H8OH-1; R: C4H6NH2-3). Post-synthetic esterification of 1 yields the acylated derivative 2, with all compounds being characterized in the solid and solution state.",

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AU - Ritchie, C.

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AB - The microwave-assisted reaction of (TBA)4[β-Mo8O24] and (TBA)3[H3V10O28] with pentaerythritol or tris(hydroxymethyl)aminomethane yields polyanions with the general formula (TBA)2[V3Mo3O16(O3-R)] (R: C5H8OH-1; R: C4H6NH2-3). Post-synthetic esterification of 1 yields the acylated derivative 2, with all compounds being characterized in the solid and solution state.

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Microwave-assisted synthesis of organically functionalized hexa-molybdovanadates

Abstract

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