Microwave assisted synthesis of a mono organoimido functionalized Anderson polyoxometalate

C. Ritchie; G. Bryant

doi:10.1039/c5dt04000k

Microwave assisted synthesis of a mono organoimido functionalized Anderson polyoxometalate

C. Ritchie, G. Bryant

Research output: Contribution to journal › Article › Research › peer-review

20 Citations (Scopus)

Abstract

The synthesis of an aliphatic organoimido functionalized polyoxometalate has been achieved through a microwave assisted reaction protocol in the absence of any activating reagents. Characterization of the pendant amine containing polyanion [Mo₆O₁₈NC(OCH₂)₃MnMo₆O₁₈(OCH₂)₃CNH₂]^5- (1) includes single crystal XRD, NMR, ESI-MS, IR and SAXS.

Original language	English
Pages (from-to)	20826-20829
Number of pages	4
Journal	Dalton Transactions
Volume	44
Issue number	48
DOIs	https://doi.org/10.1039/c5dt04000k
Publication status	Published - 1 Jan 2015
Externally published	Yes

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abstract = "The synthesis of an aliphatic organoimido functionalized polyoxometalate has been achieved through a microwave assisted reaction protocol in the absence of any activating reagents. Characterization of the pendant amine containing polyanion [Mo6O18NC(OCH2)3MnMo6O18(OCH2)3CNH2]5- (1) includes single crystal XRD, NMR, ESI-MS, IR and SAXS.",

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AB - The synthesis of an aliphatic organoimido functionalized polyoxometalate has been achieved through a microwave assisted reaction protocol in the absence of any activating reagents. Characterization of the pendant amine containing polyanion [Mo6O18NC(OCH2)3MnMo6O18(OCH2)3CNH2]5- (1) includes single crystal XRD, NMR, ESI-MS, IR and SAXS.

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Microwave assisted synthesis of a mono organoimido functionalized Anderson polyoxometalate

Abstract

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