In situ 3-D imaging of combined microstructure and crack propagation in Ti alloys using phase sensitive synchrotron microtomography

M. Karadge; L. Babout; F. Garcia-Pastor; W. Lüdwig; P. J. Withers; J. Y. Buffière; M. Preuss

In situ 3-D imaging of combined microstructure and crack propagation in Ti alloys using phase sensitive synchrotron microtomography

M. Karadge, L. Babout, F. Garcia-Pastor, W. Lüdwig, P. J. Withers, J. Y. Buffière, M. Preuss

Research output: Chapter in Book/Report/Conference proceeding › Conference Paper › Other

Abstract

It is demonstrated that phase sensitive synchrotron microtomography in the Fresnel wave propagation regime can be used to 'non-invasively and directly see in real time' the interaction between microstructure and damage mechanisms in multiphase Ti alloys. Using a combination of absorption and phase contrast imaging during in situ fatigue experiments on the ID19 micro-tomography beamline (at ESRF France), we have captured in real time some of the important microstructural damage processes occurring in two different classes of titanium alloys: Ti-6246 (Ti-6Al-2Sn-4Zr-6Mo, an α+β titanium alloy) and BurTi (Ti-2.5V-15Cr-2Al-0.2C, burn resistant β-titanium with reinforced titanium carbides). It is envisioned that this capability will prove to be a boon for further understanding the behaviour and optimization of microstructures in multiphase structural alloys.

Original language	English
Title of host publication	Ti-2007 - Proceedings of the 11th World Conference on Titanium
Editors	M. Niinomi, S. Akiyama, M. Ikeda, M. Hagiwara, K. Maruyama
Publisher	Japan Institute of Metals and Materials (JIM)
Pages	239-242
Number of pages	4
ISBN (Electronic)	9784889034066
Publication status	Published - 2007
Externally published	Yes
Event	The World Conference on Titanium 2007 - Kyoto, Japan Duration: 3 Jun 2007 → 7 Jun 2007 Conference number: 11th

Conference

Conference	The World Conference on Titanium 2007
Abbreviated title	TI 2007
Country/Territory	Japan
City	Kyoto
Period	3/06/07 → 7/06/07

Keywords

3D imaging
crack propagation
microstructure
microtomography
titanium alloys

Cite this

Karadge, M., Babout, L., Garcia-Pastor, F., Lüdwig, W., Withers, P. J., Buffière, J. Y., & Preuss, M. (2007). In situ 3-D imaging of combined microstructure and crack propagation in Ti alloys using phase sensitive synchrotron microtomography. In M. Niinomi, S. Akiyama, M. Ikeda, M. Hagiwara, & K. Maruyama (Eds.), Ti-2007 - Proceedings of the 11th World Conference on Titanium (pp. 239-242). Japan Institute of Metals and Materials (JIM).

Karadge, M. ; Babout, L. ; Garcia-Pastor, F. et al. / In situ 3-D imaging of combined microstructure and crack propagation in Ti alloys using phase sensitive synchrotron microtomography. Ti-2007 - Proceedings of the 11th World Conference on Titanium. editor / M. Niinomi ; S. Akiyama ; M. Ikeda ; M. Hagiwara ; K. Maruyama. Japan Institute of Metals and Materials (JIM), 2007. pp. 239-242

@inproceedings{fc099ff4df7b4a59b6ac417cea4ed865,

title = "In situ 3-D imaging of combined microstructure and crack propagation in Ti alloys using phase sensitive synchrotron microtomography",

abstract = "It is demonstrated that phase sensitive synchrotron microtomography in the Fresnel wave propagation regime can be used to 'non-invasively and directly see in real time' the interaction between microstructure and damage mechanisms in multiphase Ti alloys. Using a combination of absorption and phase contrast imaging during in situ fatigue experiments on the ID19 micro-tomography beamline (at ESRF France), we have captured in real time some of the important microstructural damage processes occurring in two different classes of titanium alloys: Ti-6246 (Ti-6Al-2Sn-4Zr-6Mo, an α+β titanium alloy) and BurTi (Ti-2.5V-15Cr-2Al-0.2C, burn resistant β-titanium with reinforced titanium carbides). It is envisioned that this capability will prove to be a boon for further understanding the behaviour and optimization of microstructures in multiphase structural alloys.",

keywords = "3D imaging, crack propagation, microstructure, microtomography, titanium alloys",

author = "M. Karadge and L. Babout and F. Garcia-Pastor and W. L{\"u}dwig and Withers, {P. J.} and Buffi{\`e}re, {J. Y.} and M. Preuss",

note = "Funding Information: The authors would like to thank Dr David Rugg (Rolls-Royce plc, UK) for providing the raw materials and Greg Johnson (ESRF) for experimental assistance. Financial support provided by EPSRC is also gratefully acknowledged by the authors. Funding Information: The authors would like to thank Dr David Rugg (Rolls-Royce plc, UK) for providing the raw materials and Greg Johnson ( ESRF) for experimental assistance. Financial support provided by EPSRC is also gratefully acknowledged by the authors. Publisher Copyright: {\textcopyright} Ti-2007 - Proceedings of the 11th World Conference on Titanium. All Rights Reserved.; The World Conference on Titanium 2007, TI 2007 ; Conference date: 03-06-2007 Through 07-06-2007",

year = "2007",

language = "English",

pages = "239--242",

editor = "M. Niinomi and S. Akiyama and M. Ikeda and M. Hagiwara and K. Maruyama",

booktitle = "Ti-2007 - Proceedings of the 11th World Conference on Titanium",

publisher = "Japan Institute of Metals and Materials (JIM)",

}

Karadge, M, Babout, L, Garcia-Pastor, F, Lüdwig, W, Withers, PJ, Buffière, JY & Preuss, M 2007, In situ 3-D imaging of combined microstructure and crack propagation in Ti alloys using phase sensitive synchrotron microtomography. in M Niinomi, S Akiyama, M Ikeda, M Hagiwara & K Maruyama (eds), Ti-2007 - Proceedings of the 11th World Conference on Titanium. Japan Institute of Metals and Materials (JIM), pp. 239-242, The World Conference on Titanium 2007, Kyoto, Japan, 3/06/07.

In situ 3-D imaging of combined microstructure and crack propagation in Ti alloys using phase sensitive synchrotron microtomography. / Karadge, M.; Babout, L.; Garcia-Pastor, F. et al.
Ti-2007 - Proceedings of the 11th World Conference on Titanium. ed. / M. Niinomi; S. Akiyama; M. Ikeda; M. Hagiwara; K. Maruyama. Japan Institute of Metals and Materials (JIM), 2007. p. 239-242.

Research output: Chapter in Book/Report/Conference proceeding › Conference Paper › Other

TY - GEN

T1 - In situ 3-D imaging of combined microstructure and crack propagation in Ti alloys using phase sensitive synchrotron microtomography

AU - Karadge, M.

AU - Babout, L.

AU - Garcia-Pastor, F.

AU - Lüdwig, W.

AU - Withers, P. J.

AU - Buffière, J. Y.

AU - Preuss, M.

N1 - Conference code: 11th

PY - 2007

Y1 - 2007

N2 - It is demonstrated that phase sensitive synchrotron microtomography in the Fresnel wave propagation regime can be used to 'non-invasively and directly see in real time' the interaction between microstructure and damage mechanisms in multiphase Ti alloys. Using a combination of absorption and phase contrast imaging during in situ fatigue experiments on the ID19 micro-tomography beamline (at ESRF France), we have captured in real time some of the important microstructural damage processes occurring in two different classes of titanium alloys: Ti-6246 (Ti-6Al-2Sn-4Zr-6Mo, an α+β titanium alloy) and BurTi (Ti-2.5V-15Cr-2Al-0.2C, burn resistant β-titanium with reinforced titanium carbides). It is envisioned that this capability will prove to be a boon for further understanding the behaviour and optimization of microstructures in multiphase structural alloys.

AB - It is demonstrated that phase sensitive synchrotron microtomography in the Fresnel wave propagation regime can be used to 'non-invasively and directly see in real time' the interaction between microstructure and damage mechanisms in multiphase Ti alloys. Using a combination of absorption and phase contrast imaging during in situ fatigue experiments on the ID19 micro-tomography beamline (at ESRF France), we have captured in real time some of the important microstructural damage processes occurring in two different classes of titanium alloys: Ti-6246 (Ti-6Al-2Sn-4Zr-6Mo, an α+β titanium alloy) and BurTi (Ti-2.5V-15Cr-2Al-0.2C, burn resistant β-titanium with reinforced titanium carbides). It is envisioned that this capability will prove to be a boon for further understanding the behaviour and optimization of microstructures in multiphase structural alloys.

KW - 3D imaging

KW - crack propagation

KW - microstructure

KW - microtomography

KW - titanium alloys

UR - http://www.scopus.com/inward/record.url?scp=84870707647&partnerID=8YFLogxK

M3 - Conference Paper

AN - SCOPUS:84870707647

SP - 239

EP - 242

BT - Ti-2007 - Proceedings of the 11th World Conference on Titanium

A2 - Niinomi, M.

A2 - Akiyama, S.

A2 - Ikeda, M.

A2 - Hagiwara, M.

A2 - Maruyama, K.

PB - Japan Institute of Metals and Materials (JIM)

T2 - The World Conference on Titanium 2007

Y2 - 3 June 2007 through 7 June 2007

ER -

Karadge M, Babout L, Garcia-Pastor F, Lüdwig W, Withers PJ, Buffière JY et al. In situ 3-D imaging of combined microstructure and crack propagation in Ti alloys using phase sensitive synchrotron microtomography. In Niinomi M, Akiyama S, Ikeda M, Hagiwara M, Maruyama K, editors, Ti-2007 - Proceedings of the 11th World Conference on Titanium. Japan Institute of Metals and Materials (JIM). 2007. p. 239-242

In situ 3-D imaging of combined microstructure and crack propagation in Ti alloys using phase sensitive synchrotron microtomography

Abstract

Conference

Keywords

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Cite this