Full-field energy-dispersive powder diffraction imaging using laboratory X-rays

A laboratory instrument with the ability to spatially resolve energy-dispersed X-ray powder diffraction patterns taken in a single snapshot has been developed. The experimental arrangement is based on a pinhole camera coupled with a pixelated spectral X-ray detector. Collimation of the diffracted beam is defined by the area of the footprint of a detector pixel and the diameter of the pinhole aperture. Each pixel in the image, therefore, contains an energy-dispersed powder diffraction pattern. This new X-ray imaging technique enables spatial mapping of crystallinity, crystalline texture or crystalline phases from within a sample. Validation of the method has been carried out with a back-to-back comparison with crystalline texture mapping local to a friction stir weld in an aluminium alloy taken using synchrotron radiation.