TY - JOUR
T1 - Ethyl 2-(1,3-benzodioxol-5-yl)-1-[3-(1H-imidazol-1-yl)propyl]-1H- benzimidazole-5-carboxylate
AU - Yoon, Yeong Keng
AU - Ali, Mohamed Ashraf
AU - Choon, Tan Soo
AU - Asik, Safra Izuani Jama
AU - Razak, Ibrahim Abdul
N1 - Copyright:
Copyright 2012 Elsevier B.V., All rights reserved.
PY - 2012/1
Y1 - 2012/1
N2 - In the title compound, C 23H 22N 4O 4, the essentially planar [maximum deviation = 0.022(1) Å] benzimidazole ring system forms dihedral angles of 86.16(7) and 37.38(6)°, respectively, with the imidazole and benzene rings. The dioxolane ring adopts an envelope conformation with the methylene C atom at the flap. In the crystal, C-H··· O and C-H··· N interactions link the molecules into a ribbon along the a axis. The crystal packing is further stabilized by weak π-π stacking interactions [centroid-centroid distances = 3.5954(8) and 3.7134(8) Å] and C-H··· π interactions.
AB - In the title compound, C 23H 22N 4O 4, the essentially planar [maximum deviation = 0.022(1) Å] benzimidazole ring system forms dihedral angles of 86.16(7) and 37.38(6)°, respectively, with the imidazole and benzene rings. The dioxolane ring adopts an envelope conformation with the methylene C atom at the flap. In the crystal, C-H··· O and C-H··· N interactions link the molecules into a ribbon along the a axis. The crystal packing is further stabilized by weak π-π stacking interactions [centroid-centroid distances = 3.5954(8) and 3.7134(8) Å] and C-H··· π interactions.
KW - Data-to-parameter ratio = 20.6
KW - Mean σ(C-C) = 0.002 Å
KW - R factor = 0.051
KW - Single-crystal X-ray study
KW - T = 100 K
KW - wR factor = 0.126
UR - http://www.scopus.com/inward/record.url?scp=84855387434&partnerID=8YFLogxK
U2 - 10.1107/S1600536811054572
DO - 10.1107/S1600536811054572
M3 - Article
AN - SCOPUS:84855387434
VL - 68
SP - o247-o248
JO - Acta Crystallographica Section E: Crystallographic Communications
JF - Acta Crystallographica Section E: Crystallographic Communications
SN - 2056-9890
IS - 1
ER -