TY - JOUR
T1 - Effect of β grain growth on variant selection and texture memory effect during α → β → α phase transformation in Ti-6 Al-4 v
AU - Obasi, G. C.
AU - Birosca, S.
AU - Quinta Da Fonseca, J.
AU - Preuss, M.
PY - 2012/2
Y1 - 2012/2
N2 - In the present study, the texture evolution and the role of β grain growth on variant selection during β → α phase transformation have been investigated in Ti-6 Al-4 V with and without 0.4 wt.% yttrium addition. The aim of adding yttrium was to control β grain growth above the β transus by pinning grain boundaries with yttria. Both materials were first thermomechanically processed to generate similar starting microstructures and crystallographic textures. Subsequently, both materials were solution-heat-treated above the β transus followed by slow cooling to promote growth of the α lath structure from grain boundary α. Additional interrupted slow cooling experiments were carried out to identify the α lamellae that nucleate first from β grain boundaries. Detailed electron backscatter diffraction analysis was carried out and it was found that the β heat treatment did not generate new texture components although the intensities of the individual components changed dramatically depending on the alloy/β grain size. Variant selection was assessed by comparing measured α texture components with predicted α texture components based on the high-temperature β texture assuming equal variant selection. It was found that with increasing β grain size variant selection intensified favouring the {1, Φ, 2} {90°, 30°, 0°} texture component. Interrupted cooling experiments revealed that α nucleates first on β grain boundaries that are formed by two β grains having a common (1 1 0) normal and that these α lamellae display almost exclusively a {1, Φ, 2} {90°, 30°, 0°} orientation. Consequently, the dominance of this variant with increasing β grain size can be related to the relative free growth of this particular α texture component into an "empty" β grain.
AB - In the present study, the texture evolution and the role of β grain growth on variant selection during β → α phase transformation have been investigated in Ti-6 Al-4 V with and without 0.4 wt.% yttrium addition. The aim of adding yttrium was to control β grain growth above the β transus by pinning grain boundaries with yttria. Both materials were first thermomechanically processed to generate similar starting microstructures and crystallographic textures. Subsequently, both materials were solution-heat-treated above the β transus followed by slow cooling to promote growth of the α lath structure from grain boundary α. Additional interrupted slow cooling experiments were carried out to identify the α lamellae that nucleate first from β grain boundaries. Detailed electron backscatter diffraction analysis was carried out and it was found that the β heat treatment did not generate new texture components although the intensities of the individual components changed dramatically depending on the alloy/β grain size. Variant selection was assessed by comparing measured α texture components with predicted α texture components based on the high-temperature β texture assuming equal variant selection. It was found that with increasing β grain size variant selection intensified favouring the {1, Φ, 2} {90°, 30°, 0°} texture component. Interrupted cooling experiments revealed that α nucleates first on β grain boundaries that are formed by two β grains having a common (1 1 0) normal and that these α lamellae display almost exclusively a {1, Φ, 2} {90°, 30°, 0°} orientation. Consequently, the dominance of this variant with increasing β grain size can be related to the relative free growth of this particular α texture component into an "empty" β grain.
KW - Grain growth
KW - Texture evolution
KW - Texture memory
KW - Ti-6 Al-4 V
KW - Variant selection
UR - http://www.scopus.com/inward/record.url?scp=83455218558&partnerID=8YFLogxK
U2 - 10.1016/j.actamat.2011.10.038
DO - 10.1016/j.actamat.2011.10.038
M3 - Article
AN - SCOPUS:83455218558
SN - 1359-6454
VL - 60
SP - 1048
EP - 1058
JO - Acta Materialia
JF - Acta Materialia
IS - 3
ER -