Controlled synthesis of amine-capped γ-Fe2O3 nanoparticles by a one-step process

Qingwu Peng; Jun Gan; Shufen Wang; Lingbing Kong; Guorong Chen; Yunxia Yang; Guangjian Huang

doi:10.1021/ie302148h

Controlled synthesis of amine-capped γ-Fe2O3 nanoparticles by a one-step process

Qingwu Peng, Jun Gan, Shufen Wang, Lingbing Kong, Guorong Chen, Yunxia Yang, Guangjian Huang

Research output: Contribution to journal › Article › Research › peer-review

13 Citations (Scopus)

Abstract

Amine-capped γ-Fe₂O₃ nanoparticles were prepared by a simple one-step chemical solution method. By changing the type of iron salts, the phase composition and morphology of the samples were adjusted. The resultant products were characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), transmission electron microscopy (TEM), scanning electron microscopy (SEM), and Fourier transform infrared (FTIR) spectroscopy. The magnetic properties were also studied. Triethanolamine (TEA) plays an important role in the formation of magnetic structures. It can act as a precipitator, structure-directing agent, and surface-functionalizing agent. Successful attachment of amine groups to the surface of the magnetic nanoparticles was characterized.

Original language	English
Pages (from-to)	7713-7717
Number of pages	5
Journal	Industrial and Engineering Chemistry Research
Volume	52
Issue number	23
DOIs	https://doi.org/10.1021/ie302148h
Publication status	Published - 12 Jun 2013
Externally published	Yes

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10.1021/ie302148h

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abstract = "Amine-capped γ-Fe2O3 nanoparticles were prepared by a simple one-step chemical solution method. By changing the type of iron salts, the phase composition and morphology of the samples were adjusted. The resultant products were characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), transmission electron microscopy (TEM), scanning electron microscopy (SEM), and Fourier transform infrared (FTIR) spectroscopy. The magnetic properties were also studied. Triethanolamine (TEA) plays an important role in the formation of magnetic structures. It can act as a precipitator, structure-directing agent, and surface-functionalizing agent. Successful attachment of amine groups to the surface of the magnetic nanoparticles was characterized.",

author = "Qingwu Peng and Jun Gan and Shufen Wang and Lingbing Kong and Guorong Chen and Yunxia Yang and Guangjian Huang",

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AU - Peng, Qingwu

AU - Gan, Jun

AU - Wang, Shufen

AU - Kong, Lingbing

AU - Chen, Guorong

AU - Yang, Yunxia

AU - Huang, Guangjian

PY - 2013/6/12

Y1 - 2013/6/12

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AB - Amine-capped γ-Fe2O3 nanoparticles were prepared by a simple one-step chemical solution method. By changing the type of iron salts, the phase composition and morphology of the samples were adjusted. The resultant products were characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), transmission electron microscopy (TEM), scanning electron microscopy (SEM), and Fourier transform infrared (FTIR) spectroscopy. The magnetic properties were also studied. Triethanolamine (TEA) plays an important role in the formation of magnetic structures. It can act as a precipitator, structure-directing agent, and surface-functionalizing agent. Successful attachment of amine groups to the surface of the magnetic nanoparticles was characterized.

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JO - Industrial and Engineering Chemistry Research

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Controlled synthesis of amine-capped γ-Fe2O3 nanoparticles by a one-step process

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