TY - JOUR
T1 - Comprehensive two-dimensional gas chromatography with flame ionization and time-of-flight mass spectrometry detection
T2 - Qualitative and quantitative analysis of west Australian sandalwood oil
AU - Shellie, Robert
AU - Marriott, Philip
AU - Morrison, Paul
PY - 2004/1/1
Y1 - 2004/1/1
N2 - The use of gas chromatography (GC)-mass spectrometry (MS), GC-time-of-flight MS (TOFMS), comprehensive two-dimensional GC (GC×GC)-flame ionization detection (FID), and GC×GC-TOFMS is discussed for the characterization of the eight important representative components, including Z-α-santalol, epi-α-bisabolol, Z-α-trans-bergamotol, epi-β-santalol, Z-β-santalol, E,E-farnesol, Z-nuciferol, and Z-lanceol, in the oil of west Australian sandalwood (Santalum spicatum). Single-column GC-MS lacks the resolving power to separate all of the listed components as pure peaks and allow precise analytical measurement of individual component abundances. With enhanced peak resolution capabilities in GC×GC, these components are sufficiently well resolved to be quantitated using flame ionization detection, following initial characterization of components by using GC×GC-TOFMS.
AB - The use of gas chromatography (GC)-mass spectrometry (MS), GC-time-of-flight MS (TOFMS), comprehensive two-dimensional GC (GC×GC)-flame ionization detection (FID), and GC×GC-TOFMS is discussed for the characterization of the eight important representative components, including Z-α-santalol, epi-α-bisabolol, Z-α-trans-bergamotol, epi-β-santalol, Z-β-santalol, E,E-farnesol, Z-nuciferol, and Z-lanceol, in the oil of west Australian sandalwood (Santalum spicatum). Single-column GC-MS lacks the resolving power to separate all of the listed components as pure peaks and allow precise analytical measurement of individual component abundances. With enhanced peak resolution capabilities in GC×GC, these components are sufficiently well resolved to be quantitated using flame ionization detection, following initial characterization of components by using GC×GC-TOFMS.
UR - http://www.scopus.com/inward/record.url?scp=4644298833&partnerID=8YFLogxK
U2 - 10.1093/chromsci/42.8.417
DO - 10.1093/chromsci/42.8.417
M3 - Article
C2 - 15516281
AN - SCOPUS:4644298833
SN - 0021-9665
VL - 42
SP - 417
EP - 422
JO - Journal of Chromatographic Science
JF - Journal of Chromatographic Science
IS - 8
ER -